Dr. R. Fernandez-Ruiz (Universidad Autonoma de Madrid, Spain) recently published a theoretical paper on the expanded uncertainty associated with TXRF measurements. For more information, see the paper, "Uncertainty in the Multielemental Quantification by Total-Reflection X-ray Fluorescence: Theoretical and Empirical Approximation", R. Fernandez-Ruiz, Anal. Chem., 80, 8372-8381 (2008).
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